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Characterization included spectroscopic ellipsometry, scanning electron microscopy (SEM), transmission electron microscopy (TEM) with electron energy loss spectroscopy (EELS) and selected area electron diffraction (SAED), X-ray diffraction (XRD), thermogravimetric analysis (TGA), N 2 adsorption-desorption analysis, and Fourier transform infrared spectroscopy (FTIR)

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Lipid peroxidation products such as oxidized phosphatidylethanolamine (PEox) generate hydroxyl radicals through the Fenton reaction, which directly damage cell membrane integrity and release toxic aldehydes (such as malondialdehyde, MDA) (172)