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Following the above general alkylation reaction (procedure C) the crude reaction mixture was purified by column chromatography (dichloromethane:methanol=100:1) to provide the desired ethyl 3-(benzylamino)-4-(2 adamantylamino)-benzoate (SRS15-20_mono, Scheme 2) (19 mg, 0.047 mmol, 50%) and the dialkylation compound, the ethyl 3-(dibenzylamino)-4-(2-adamantylamino)-benzoate, (SRS15-20_di, Scheme 2) (9 mg, 0.018 mmol, 19%)

Metabolic regulation and the anti-obesity perspectives of human brown fat

Fuchs CS, Azevedo S, Okusaka T, Van Laethem J-L, Lipton LR, Riess H, et al

Functional characterization of a basic helix-loop-helix (bHLH) transcription factor GhDEL65 from cotton ( Gossypium hirsutum )